1. Extreme Ultraviolet Optics

Pushing Optics to the Extreme

 

New tabletop sources make applications from 10-100nm more accessible

 

EUV applications include metrology, nanoscale imaging, and electron spectroscopy

 

EUV systems often use reflective optics as high absorption makes refraction impractical

 

Surface roughness is critical because scatter is much higher at shorter wavelengths

Extreme ultraviolet (EUV) radiation encompasses the band of wavelengths from roughly 10nm to 100nm, between the X-ray and deep UV (DUV) spectral regions. With numerous pressing applications in the EUV region including lithography, nanoscale imaging, and spectroscopy, much effort has recently been focused on developing compact EUV sources. That effort has led to the commercial availability of several types of EUV light sources.

EUV radiation is absorbed strongly in nearly all materials, so optical components are almost always reflective, not transmissive. Because the wavelength is short, EUV optics have surface quality requirements that are more demanding than those for visible-light components. While producing EUV optics is not easy due to their demanding requirements, it is worth the effort because of the benefits of utilizing EUV radiation for high resolution imaging, spectroscopy, and materials processing.

EUV Radiation Sources

The first practical EUV radiation sources were huge devices available only to large research labs and lithography companies, but recent advancements in EUV technology has made way for much smaller and more accessible tabletop EUV systems. High Harmonic Generation (HHG) systems and capillary discharge lasers are two of the more promising new EUV tabletop sources, producing beams of coherent radiation with low divergence.

Applications for EUV Optics

New compact EUV sources are spawning a multitude of emerging EUV applications including high resolution imaging, electron spectroscopy, molecular and solid state dynamics research, and nano-machining.

EUV Imaging

EUV radiation is ideal for coherent diffractive imaging (CDI), an imaging technique capable of achieving resolutions down to 0.5nm. CDI is used for analyzing extremely small structures such as nanotubes and nanocrystals. In CDI, mirrors are used to direct an EUV beam onto an object. Features on, or even below the surface diffract the radiation which is then captured on a nearby CCD detector. The recorded diffraction pattern is then processed in software, producing a 2D or 3D image of the original object. Because mirrors and diffraction are utilized instead of transmissive lenses, the final image is nearly diffraction limited and free of almost all aberrations. Diffraction limited resolution is directly proportional to wavelength, so the short wavelengths of EUV radiation further improve resolution. CDI is a non-contact imaging technique that is faster than similar techniques such as atomic force microscopy, capturing images in around one minute. The high resolution made available by EUV CDI is pushing the current limits of imaging technology.

Typical EUV coherent diffractive imaging setup
Figure 1: Typical EUV coherent diffractive imaging setup

EUV Optical and Photoelectron Spectroscopy

EUV spectroscopy can probe energy levels that are not accessible using other spectroscopy techniques, making it valuable for many research applications. EUV radiation is used in photoemission spectroscopy, which determines the energies of electrons in a solid, liquid or gas by measuring the energy of electrons emitted by the photoelectric effect. EUV spectroscopy is also used in nuclear fusion research, as the radiation emitted from most plasma impurities found in fusion experiments falls between 1-50nm. The short wavelengths of EUV radiation can also allow EUV spectroscopy systems to determine the exact location of specific elements in a structured object. Research enabled by EUV spectroscopy has the potential to make a substantial impact on materials science and energy sources utilizing nuclear fusion.

EUV radiation falls between X-ray and ultraviolet spectral regions
Figure 2: EUV radiation falls between the X-ray and ultraviolet spectral regions

EUV Nano-Machining

The ability to machine smaller and smaller microsctructures and nanostructures is critical to the development of nanotechnology. EUV nano-machining is still in the very early stages of development, but is a promising technique for generating and modifying nanometer-scale structures. Focused spot size is directly proportional to wavelength, therefore EUV nano-machining systems have a higher spatial resolution than systems utilizing longer wavelengths. The short absorption depth of EUV radiation in most materials also results in localization of the energy, facilitating the etching of extremely fine features. Nanotechnology has the potential to make a significant impact on society, improving medical devices and procedures, manufacturing methods, energy systems, electronics, and more.

Nano-machining is a critical part of a number of emerging applications
Figure 3: Nano-machining is a critical part of a number of emerging applications including nanoelectronics, nanomedicine, and biomaterials

Optical Components for EUV Applications

EUV systems need to be contained in a vacuum because wavelengths below 100nm cannot be transmitted through air. Similarly, EUV radiation has extremely high absorption in almost all materials, so optical components in EUV applications are nearly always reflective. Scatter is higher at short wavelengths, which makes surface roughness, surface flatness, and other surface tolerances important for EUV optics. A common type of mirror used in EUV applications is the multilayer Bragg mirror, where a periodic stack of two different materials causes a specific band of wavelengths to constructively interfere and reflect. Part of the incident beam is reflected at each interface in the stack. EUV multilayer mirrors have a very narrow bandwidth, on the order of 1nm, requiring EUV optics of this type to be specifically matched to the wavelength of the source.

Example of a λ/4 Bragg reflector that could be used as an EUV mirror
Figure 4: Structure of a λ/4 multilayer mirror. EUV mirrors typically have about 50 pairs of layers.
 

Extreme Ultraviolet Optics at Edmund Optics®

Extreme Ultraviolet (EUV) Flat Mirrors Extreme Ultraviolet (EUV) Flat Mirrors

Extreme Ultraviolet (EUV) Flat Mirrors are multilayer Bragg reflectors with reflective coatings deposited on a super-polished single crystal silicon substrate resulting in a surface roughness less than 3Å. They are designed for maximum achievable reflectance at their design wavelength and angle of incidence. The mirrors are available with either a 5° or 45° angle of incidence (AOI).

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Extreme Ultraviolet (EUV) Flat Mirrors Extreme Ultraviolet (EUV) Spherical Mirrors

Extreme Ultraviolet (EUV) Spherical Mirrors feature multilayer Mo/Si coatings just like the Extreme Ultraviolet (EUV) Flat Mirrors, but they utilize a curved substrate for focusing unpolarized EUV sources at a 5° angle of incidence. They offer >60% reflection at 13.5nm, a <3Å RMS surface roughness, and narrow pass band of 0.5nm.

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FAQ's

FAQ  Why are the Extreme Ultraviolet (EUV) Flat Mirrors designed for 13.5nm?
The Extreme Ultraviolet (EUV) Flat Mirrors are designed for use at 13.5nm because 13.5nm is one of the most commonly used EUV wavelengths. Tin-plasma sources used for lithography emit at 13.5nm, and other EUV applications are also adopting this wavelength as the standard.
FAQ  Why do the Extreme Ultraviolet (EUV) Flat Mirrors use single crystal silicon substrates and not fused silica?

While some EUV optics use fused silica substrates, EO offers Extreme Ultraviolet (EUV) Flat Mirrors with single crystal silicon substrates due to their superior thermal stability compared to fused silica.

FAQ  Why can’t transmissive optics be used with EUV radiation?

EUV photons have an energy of around 90eV; the typical ionization energies of organic materials and metals are 7-9eV and 4-5eV respectively. Consequently, EUV photons are easily absorbed, generating photoelectrons and secondary electrons which prevents EUV radiation from transmitting through virtually all materials.

FAQ   How are images produced in coherence diffraction imaging (CDI) if the light scattering off of the sample is not focused back down into an image on the CCD detector?

The radiation scattering off of the object creates a reciprocal space diffraction pattern on the detector. An inverse Fourier transform algorithm is applied to the recorded pattern to reconstruct an image. Instead of using a lens system to form an image on a detector, software is used to convert the scattered diffraction pattern into a height map of the object.

Resources

Application Notes

Technical information and application examples including theoretical explanations, equations, graphical illustrations, and much more.

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